Delta F Platinum Series Manual de usuario

Platinum Series

Process Oxygen Analyzer

Instruction Manual

P/N 99000001

DELTA F CORPORATION

4 Constitution Way !Woburn, Massachusetts 01801-1087

Telephone: (781) 935-4600 !FAX: (781) 938-0531

Platinum Series

Process Oxygen Analyzer

Instruction Manual

P/N 99000001

Revision G

Covers Firmware

Version 2.82 And Higher

DELTA F CORPORATION

4 Constitution Way

Woburn, MA 01801-1087

Telephone: 781-935-4600

FAX: 781-938-0531

Service Dept.: 781-935-5808

Service FAX: 781-932-0053

This entire publication and/or its' PDF version may be reproduced, transmitted, and

stored electronically. Note that this manual must only be reproduced, transmitted or

stored in its’ entirety. Extraction of a portion of the printed or the PDF document, for

any use, requires written permission from Delta F Corporation.

Stablex, Bi-Strata, and NanoTrace are trademarks of Delta F Corporation. VCR®is a

registered trademark of the Cajon Company. Waferpure™ is a trademark of Millipore

Corporation. Nanochem®is a registered trademark of Semigas Corporation. Snoop®is

a registered trademark of Nupro Company. MicroTorr™ is a registered trademark of

SAES.

DELTA F CORPORATION

Platinum Series Process Oxygen Analyzer Instruction Manual

Table Of Contents iii

TABLE OF CONTENTS

1.0 Overview Of This Manual .......................................1-1

1.1 Introduction ................................................1-2

1.2 Definitions And Warnings .....................................1-2

1.2.1 Explanation Of Graphic Symbols .........................1-2

1.2.2 Definitions ..........................................1-5

1.3 Unpacking .................................................1-6

1.4 Verify Operating Voltage ......................................1-7

2.0 Quick Set-up Procedure ........................................2-1

2.1 Tools Required ..............................................2-1

2.2 Adding The Electrolyte ........................................2-1

2.3 Sample Gas Connections .....................................2-3

2.4 Electrical Connections ........................................2-3

2.5 Standard Outputs ............................................2-3

2.6 Powering Up ...............................................2-4

2.7 Operational Recommendations .................................2-6

3.0 Beyond The Basic Analyzer - The Options .........................3-1

3.1 High-Resolution Model ........................................3-2

3.2 STAB-EL ..................................................3-3

3.3 Pump .....................................................3-3

3.4 Heater ....................................................3-4

3.5 Installation Of The Filter .......................................3-6

3.6 Installation Of The Pressure Regulator ...........................3-7

3.7 Installation Of Both Filter And Pressure Regulator ..................3-8

3.8 Supplemental Ni-Cd Battery Power ..............................3-9

3.9 Key Lock ..................................................3-9

3.10 Stainless Steel Outlet Line ...................................3-10

3.11 Welded Gas Delivery System With VCR®Metal Face-Seal Inlet

Connections ............................................3-10

3.12 4-20 mA Fully Isolated Output ................................3-11

3.13 Quick Start ...............................................3-12

3.14 Password Protection .......................................3-12

3.15 Gas Scale Factor ..........................................3-12

3.16 Alarms ..................................................3-12

3.16.1 Oxygen Alarms .....................................3-12

3.16.2 Temperature Alarm .................................3-13

3.16.3 Low Flow Alarm ....................................3-13

3.16.4 Electrolyte Condition Alarm ...........................3-13

DELTA F CORPORATION

Platinum Series Process Oxygen Analyzer Instruction Manual

Table Of Contentsiv

3.17 Expanded Range Scale Output ...............................3-13

3.18 Relay Contact Closures .....................................3-14

3.19 Panel/Rack Mount .........................................3-14

3.20 Comm Ports ..............................................3-14

4.0 Connecting To External Devices .................................4-1

4.1 Introduction ................................................4-1

4.2 The Comm Port .............................................4-1

4.3 Relay Ports ................................................4-2

4.4 Sensor Port ................................................4-3

4.5 Option Ports ................................................4-4

4.6 Changing The Analog Voltage Output Selection ....................4-5

4.7 Proper Grounding & Cable Shielding For External Equipment .........4-7

4.7.1 Output Signal Grounding ...............................4-7

4.7.2 Cable Shielding ......................................4-9

4.7.3 Hook-up For Specific Analyzer Configurations ..............4-11

4.7.3.1 Standard Analyzer With No RS-232, RS-485, Or

Isolated 4-20 mA Options .......................4-11

4.7.3.2 Analyzer With Optional 4-20 mA, But No RS-232 Or

RS-485 ......................................4-12

4.7.3.3 Analyzer With Optional RS-232 ..................4-13

4.7.3.4 Analyzer With Optional RS-485 ..................4-14

5.0 Gas Sample Preparation And Delivery .............................5-1

5.1 Sample Flow Rate And Pressure ................................5-1

5.1.1 Flow Rate Effects On Sensor Performance .................5-1

5.1.2 Background Gas Effects On Indicated Flow Rate ............5-2

5.1.2.1 Indicated Flow Corrections For H2Or He ............5-2

5.1.3 Positive Pressure Operation .............................5-3

5.1.4 Negative Pressure Operation ............................5-4

5.1.5 Pressure Effects On Sensor Performance ..................5-5

5.2 Gas Sample Compatibility .....................................5-5

5.2.1 Condensation / Liquid Slugs ............................5-6

5.2.2 Gas Solubility In Aqueous KOH Solution ...................5-7

5.2.3 Reactivity With KOH Electrolyte ..........................5-7

5.2.4 Sample Gas Flammability ..............................5-7

5.2.5 Abnormal Process Condition Or Maintenance Operation ......5-8

5.2.6 Capability Of The STAB-EL System ......................5-8

5.3 Normal Installation And Operation Considerations .................5-10

5.3.1 Normal Operating Conditions ...........................5-10

5.3.2 Sample Gas Temperature Control .......................5-11

5.3.3 Back Pressure/Sample Outlet Vent ......................5-11

5.3.4 Checking For Plumbing Leaks ..........................5-12

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Platinum Series Process Oxygen Analyzer Instruction Manual

Table Of Contents v

5.4 Sampling Considerations During Calibration ......................5-12

5.4.1 Calibration Standards .................................5-13

5.4.2 Cylinder Regulators ..................................5-13

5.4.3 Process Conditions During Calibration ....................5-15

5.4.3.1 Delivery And Vent Pressure During Calibration ......5-15

5.4.3.2 Background Gas Effects On Calibration ............5-15

6.0 User Interface .................................................6-1

6.1 Introduction ................................................6-1

6.2 The Main Menu .............................................6-4

6.2.1 Programming Protocol .................................6-5

6.3 Controls ...................................................6-7

6.3.1 Quick St(art) .........................................6-7

6.3.2 Pump ..............................................6-8

6.3.3 Heater .............................................6-8

6.3.4 Sensor Polarization ...................................6-8

6.3.5 SensOFF Relay ......................................6-9

6.3.6 P(o)w(e)r UP .......................................6-10

6.3.7 ESC ..............................................6-10

6.4 Set-Up ...................................................6-10

6.4.1 Alarms ............................................6-11

6.4.1.1 O2Alarms ...................................6-12

6.4.1.2 Temperature Alarm ...........................6-14

6.4.1.3 Low Flow Alarm ..............................6-14

6.4.1.4 Electrolyte Condition Alarm .....................6-15

6.4.2 Analog Outputs .....................................6-15

6.4.2.1 Scaling Analog Output Range On High-Resolution

Analyzers ....................................6-16

6.4.2.2 Expanded Range Scale Operation And Setup .......6-19

6.4.2.3 ExpRng Relay ................................6-20

6.4.2.4 CAL FREEZE ................................6-20

6.4.2.5 IN-CAL RELAY ...............................6-20

6.4.3 Comm Port .........................................6-20

6.4.3.1 Port ........................................6-21

6.4.3.2 Device ID:xxx ................................6-21

6.4.3.3 Baud .......................................6-21

6.4.3.4 Update And Quit ..............................6-22

6.4.4 GSF ..............................................6-22

6.4.5 Oxygen Calibration ...................................6-22

6.4.5.1 Background Gas Correction .....................6-22

6.4.5.2 Check/Adj Span ..............................6-26

6.4.5.3 Reset Orig(inal) Span ..........................6-29

6.4.5.4 New Sensor .................................6-30

DELTA F CORPORATION

Platinum Series Process Oxygen Analyzer Instruction Manual

Table Of Contentsvi

6.5 The Password Menu ........................................6-30

6.6 Diagnostics ...............................................6-33

6.6.1 Prescaler ..........................................6-33

6.6.2 Sensor Temperature .................................6-33

6.6.3 Sensor Zero ........................................6-34

6.6.3.1 ZERO REF ..................................6-35

6.6.3.2 Reset Orig(inal) Zero ..........................6-35

6.6.3.3 Zero Cal(ibration) .............................6-35

6.6.4 Test Output ........................................6-38

6.6.5 Test Relays ........................................6-38

6.6.6 Memory Test .......................................6-39

6.6.7 Screen Test ........................................6-39

7.0 Theory Of Operation ...........................................7-1

7.1 The Sensor ................................................7-1

7.2 The STAB-EL Electrolyte System ...............................7-1

7.2.1 STAB-EL And Carbon Dioxide ...........................7-3

7.2.2 STAB-EL And Gases In The Halogen Family ...............7-3

7.2.3 STAB-EL With Organic, Nitrogen, Or Sulfur Containing Acid

Gases .............................................7-3

7.3 The Gas Scale Factor ........................................7-3

7.4 Effects Of Gas Sample Flow Rate On Sensor Performance ...........7-5

7.5 Pressure Effects On Sensor Performance .........................7-5

7.6 Temperature Effects On Sensor Performance .....................7-6

7.6.1 Determining Maximum Temperature Effects On Analyzer

Readings ..........................................7-6

8.0 Service ......................................................8-1

8.1 Maintenance ...............................................8-1

8.1.1 Calibration ..........................................8-1

8.1.2 Storage Temperature ..................................8-2

8.1.3 Sensor Maintenance ..................................8-2

8.1.4 Replacing The Filter ...................................8-4

8.2 Troubleshooting .............................................8-4

8.2.1 Sample System Leak Test (Low Flow Sensitivity) ............8-4

8.2.2 Basic Troubleshooting .................................8-6

8.3 Shipping ..................................................8-10

9.0 Safety .......................................................9-1

9.1 General Warnings ...........................................9-1

9.2 Electrolyte Material Safety Data Sheet (MSDS) .....................9-3

DELTA F CORPORATION

Platinum Series Process Oxygen Analyzer Instruction Manual

Table Of Contents vii

10.0 Specifications ................................................10-1

11.0 Warranty ....................................................11-1

Appendix A - Replaceable Spare Parts List ............................. A-1

Index ............................................................. I-1

DELTA F CORPORATION

Platinum Series Process Oxygen Analyzer Instruction Manual

Table Of Contentsviii

LIST OF FIGURES

Figure 1-1: Delta F Platinum Series Process Oxygen Analyzer ...............1-3

Figure 1-2: Major Internal Components ..................................1-4

Figure 2-1: Quick Disconnect Fitting At Rotameter Outlet ....................2-2

Figure 2-2: Pinouts At Enclosure Rear ..................................2-4

Figure 2-3: Front Panel Display, Main Menu ..............................2-5

Figure 3-1: Plumbing Configurations ....................................3-5

Figure 3-2: Filter Installation ..........................................3-6

Figure 3-3: Regulator Installation ......................................3-7

Figure 3-4: Filter And Regulator Installation ..............................3-8

Figure 3-5: Rack Mount Configuration ..................................3-15

Figure 3-6: Panel Mount Configuration .................................3-15

Figure 3-7: Cutout Dimensions For Panel Mount .........................3-16

Figure 4-1: Ground Loop Example .....................................4-8

Figure 4-2: Analyzer Internal Grounding .................................4-9

Figure 4-3: Analyzer With Relay Outputs ...............................4-10

Figure 4-4: Standard Analyzer Outputs (No RS-232, RS-485, Or Isolated

4-20 mA Option ..........................................4-11

Figure 4-5: Analyzer With Optional Isolated 4-20 mA (No RS-232 Or RS-485

Option) ................................................4-12

Figure 4-6: Analyzer With Optional RS-232 And Optional Isolated 4-20 mA,

If Equipped .............................................4-13

Figure 4-7: Analyzer With Optional RS-485 And Optional Isolated 4-20 mA,

If Equipped .............................................4-14

Figure 6-1: Data Display Screen .......................................6-1

Figure 6-2: Main Menu ..............................................6-4

Figure 6-3: Menu Tree - Operator Interface ..............................6-6

Figure 6-4: Control Menu ...........................................6-7

Figure 6-5: Set-Up Menu ..........................................6-11

Figure 6-6: Alarm Selection Menu ...................................6-11

Figure 6-7: Oxygen Alarm Selection Menu .............................6-12

Figure 6-8: Alarm Set-Up Screen (Alarm Not Used) ......................6-12

Figure 6-9: Alarm Set-Up Screen (Alarm Used) .........................6-13

Figure 6-10: Recorder Output Set-Up Menu ............................6-15

Figure 6-11: Recorder Output Scaling For High-Resolution Analyzers ..........6-17

Figure 6-12: Comm Port Set-Up Menu .................................6-21

Figure 6-13: Oxygen Cal Menu .......................................6-22

Figure 6-14: Gas Scale Factor Menu .................................6-23

Figure 6-15: Gas Scale Factor Menu (cont.) ............................6-24

Figure 6-16: Span Check Menu ......................................6-26

Figure 6-17: Calibration Converging Screen ............................6-28

Figure 6-18: Oxygen Cal Menu After User’s Calibration ....................6-29

DELTA F CORPORATION

Platinum Series Process Oxygen Analyzer Instruction Manual

Table Of Contents ix

Figure 6-19: Password Menu ........................................6-31

Figure 6-20: Password Entry Screen ..................................6-32

Figure 6-21: Diagnostics Menu .......................................6-33

Figure 6-22: Sensor Zero Menu ......................................6-34

Figure 6-23: Zero Cal Warning Screen .................................6-35

Figure 6-24: Zero Cal Screen ........................................6-36

Figure 6-25: Zero Cal, Not Stable Yet Screen ...........................6-37

Figure 6-26: Output Test Screen .....................................6-38

Figure 6-27: Relay Test Screen ......................................6-38

Figure 6-28: Memory Test Screen ....................................6-39

Figure 7-1: Diagram Of The Sensor Configuration .........................7-3

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