CETAC ASXpress Manual de usuario

CETAC

ASXPRESS

Rapid Sample Introduction System

Operator’s Manual

Manual Part Number 480166Rev 4

Technologies

480166 Rev 4 , April, 2010

REPRODUCTION

transmission of this document in whole or in

part, and by any means without the express

written consent of the copyright owner or

authorized agent is prohibited. Requests for

additional copies of this, or any other CETAC

publication, can be filled by contacting an

authorized distributor or

CETAC Technologies

Customer Service & Support

14306 Industrial Road

Omaha, Nebraska 68144, USA

Phone (800) 369-2822 (USA only)

Phone (402) 733-2829

Fax (402) 733-1932

E-mail custserv@cetac.com

DISCLOSURE

This document contains CETAC proprietary

data and is provided solely to its customers

for their express benefit of safe, efficient

operation and maintenance of the product

described herein. Use or disclosure of CETAC

proprietary data for the purpose of

manufacture or reproduction of the item

described herein, or any similar item is

prohibited, and delivery of this document

shall not constitute any license or implied

authorization to do so.

REVISIONS

CETAC Technologies strives to provide the

scientific community with an unparalleled

combination of effective technology and

continuing value. Modular upgrades for

existing instruments will continue to be a

prime consideration as designs progress.

CETAC Technologies reserves the right to

revise this document and/or improve

products described herein at any time without

notice or obligation. Warranty registration

entitles the named owner exclusively to

manual change pages/new editions as they

are published.

SAFETY

Instruments, accessories, components or

other associated materials may not be

returned to CETAC Technologies if

contaminated with biohazard or radioactive

materials, infectious agents, or any other

materials and/or conditions that could

constitute a health or injury hazard to CETAC

employees. Call Customer Service and

Support if there is any question or doubt

relative to decontamination requirements.

CAUTION and WARNING statements, as

applied in this document, shall be interpreted

consistent with the following context:

CAUTION applies only to potential property

damage conditions; WARNING applies to

potential personal injury conditions, in

combination with or exclusive of potential

property damage.

All user-serviceable components are

specifically identified in this document as

such; the balance shall be assumed to require

the expertise of a factory service

technician/engineer for adjustment, repair,

replacement, modification, etc. Others not so

qualified and performing these actions shall

do so at their own risk.

ORIGINAL PACKAGING

Furthermore, never

operate the instrument without first reading

and understanding the Operator’s Manual and

ensuring that the instrument is operated

safely and properly.

Retain original factory packaging for moves

and factory return shipments. Shipping in

anything other than the original fitted foam

and container can result in incidental damage

from which the purchaser will not be

protected under warranty.

TRADEMARK ACKNOWLEDGEMENTS

Windows is a registered trademark of

Microsoft Corporation in the United States and

other countries.

All other marks are the property of their

respective owners.

Under all conditions the user must observe safe laboratory procedures

during the operation of this product.

WARNING

Contents

ASXpress Rapid Sample Introduction System Operator’s Manual

Preface

1Contents

1Contents ......................................................................................................................4

1Introduction ..............................................................................................................8

Overview ....................................................................................................................................8

1.1 Rapid Sample Introduction System Standard Components ....................10

1.2 Optional Accessories/Components ....................................................................13

1.3 About This Book..........................................................................................................14

1.3.1 Who Should Read This Book.................................................................. 14

Where to Go for More Information..............................................................................14

2Preparing for Installation..................................................................................16

2.1 Choosing a Location ..................................................................................................16

2.1.1 Space Requirements.................................................................................. 16

2.1.2 Liquid Waste Routing Requirements ................................................. 16

2.1.3 Power Requirements................................................................................. 17

2.2 Unpacking the ASXpress Rapid Sample Introduction System................17

3Installing the ASXPRESS Rapid Sample Introduction System..................20

3.1 Prepare the CETAC Autosampler ........................................................................21

3.1.1 Install the Auxiliary I/O Connector Card and Processor (Rabbit)

Module..................................................................................................................... 22

3.1.2 Continuation of I/O board and “Rabbit” module installation for

CETAC autosampler ASX-520/ASX-520HS ............................................... 32

3.1.3 Continuation of I/O board and “Rabbit” module installation for

CETAC ASX-260 autosampler......................................................................... 38

3.1.4 Increase the Peristaltic Pump Speed Setting .................................. 49

3.1.5 Internal work is complete; replace all covers, etc......................... 51

3.1.6 Install the Standard-Bowl Rinse Station and Modified Rinse

Tubing Arrangement......................................................................................... 52

3.1.7 Install the 1.0mm ID Sample Probe on the Autosampler ........... 56

3.2 Connect the ASXPRESS system ................................................................................57

3.2.1 Connect the ASXPRESS Plumbing........................................................... 57

3.2.2 Connect the Electronics Module to the Valve/Pump Module ... 60

3.2.3 Connect the ASXPRESS system to the Autosampler ........................ 61

3.2.4 Connect the Autosampler to the Host Computer........................... 62

3.3 Install the ASXPRESS Software ................................................................................63

3.4 Upgrade the Firmware on the Autosampler...................................................70

3.4.1 Autosampler Programming Configuration ..................................... 70

3.4.2 Load the Firmware Upgrade, via the Rabbit Field Utility (RFU)

program, from the CD provided.................................................................... 72

4Verifying Installation/ Function Overview .................................................82

Testing the Interface..........................................................................................................82

4.1.1 To test the communications interface, complete the following

steps:........................................................................................................................ 83

4.2 Function Overview.....................................................................................................86

4.3 Operation Controls ....................................................................................................86

4.3.1 Enable ASXpress Operation.................................................................... 86

4.3.2 Enable Vacuum Pump Timeout............................................................ 87

4.4 Additional Xpress Configuration Tool Features ...........................................87

4.4.1 Notes Window ............................................................................................. 87

ASXpress Rapid Sample Introduction System Operator’s Manual

Preface

4.5 Regular Inspection of ASXPRESS Components .................................................88

5Using the Rapid Sample Introduction System ........................................... 90

5.1 Establishing Optimal Operating Conditions....................................................90

5.1.1 Creating the Lab Environment .............................................................90

5.1.2 Replacing Rapid Sample Introduction System Components .....91

5.1.3 Purchasing Supplies ..................................................................................91

5.1.4 Starting the ASXPRESS Rapid Sample Introduction System.......92

5.2 Shutting Down the ASXPRESS Rapid Sample Introduction System.........93

5.3 Flushing the Rinse Station and Flow Path .......................................................94

6Maintaining the ASXPRESS Rapid Sample Introduction System............ 96

6.1 Cleaning the Rapid Sample Introduction System .........................................96

6.1.1 Daily External Cleaning...........................................................................96

6.1.2 6-Port Valve Cleaning...............................................................................96

6.2 Checking for Leaks .....................................................................................................99

6.3 Replacing the Tubing.................................................................................................99

6.4 6-Port Valve Replacement or Reorientation................................................100

7Troubleshooting the Rapid Sample Introduction System...................104

7.1 Power System Problems.......................................................................................104

7.2 Interface Problems..................................................................................................106

7.2.1 RS-232 Cable Problems ......................................................................... 106

7.2.2 USB cable Problems................................................................................ 106

7.2.3 Software Configuration Problems .................................................... 106

7.3 Returning the Product to CETAC for Service...............................................109

7.3.1 Shipping the Product ............................................................................. 109

7.3.2 Product Warranty Statement............................................................. 109

7.3.3 Returned Product Procedures ............................................................ 110

7.3.4 Returned Product Warranty Determination................................ 111

8Glossary .................................................................................................................114

9Guide to Operating a CETAC Autosampler Using a Terminal Program

...................................................................................................................................116

9.1 Using C-Term™..........................................................................................................116

9.1.1 Starting C-Term ....................................................................................... 116

9.1.2 Overview of the C-Term Window ...................................................... 116

9.1.3 Configuring C-Term................................................................................ 117

9.1.4 Setting Preferences................................................................................. 118

9.2 Using HyperTerminal.............................................................................................119

9.3 Autosampler Commands ......................................................................................123

10 Safety and Regulatory Information .............................................................126

10.1 Characteristics..................................................................................................126

10.1.1 Environmental Characteristics .................................................... 126

10.1.2 Electrical Characteristics ............................................................... 126

10.2 Safety Notices ...................................................................................................128

10.2.1 Mains Disconnect............................................................................... 128

10.2.2 Cleaning Instructions....................................................................... 129

10.2.3 Operating Environment .................................................................. 129

10.2.4 Explanation of Caution and Warning Notices ....................... 129

10.3 Avertissements en Français .......................................................................131

10.4 Electromagnetic Interference....................................................................132

ASXpress Rapid Sample Introduction System Operator’s Manual

Preface

10.5 Explanation of Regulatory Marks............................................................ 132

11 Index....................................................................................................................... 134

Introduction

ASXpress Rapid Sample Introduction System Operator’s Manual

Chapter 1: Introduction

1Introduction

Overview

The CETAC Technologies ASXPRESS Rapid Sample Introduction System is

designed to increase autosampler throughput by reducing the sample delivery,

stabilization, and washout time (See Figure 1-1 and Figure 1-2 for cycle

diagrams). The CETAC ASXPRESS uses a combination of a metal-free 6-port

injection valve with an inert high-speed vacuum pump to enable rapid sample

loading and probe wash out. The small footprint allows placement in close

proximity to the nebulizer to provide quick sample input. The system is

sturdy, reliable, and easy to use.

The complete ASXPRESS system is comprised of 4 components:

•The ASXPRESS valve/pump module

•The ASXPRESS electronics module

•A CETAC ASX-260, ASX-520, ASX-520HS or EXR-8 autosampler with

specialized firmware

•Windows-based software to allow the configuration of the system

The ASXPRESS system is connected to, powered, and controlled by a CETAC

autosampler. The ASXPRESS system is operated by the autosampler executing a

macro automatically when the probe is placed into the sample. The macro

ends when the probe is lifted out of the rinse station. .

ASXpress Rapid Sample Introduction System Operator’s Manual

Chapter 1: Introduction

Figure 1-1 “Load Sample” Cycle Diagram

Figure 1-2 “Inject/Rinse” Cycle Diagram

ASXpress Rapid Sample Introduction System Operator’s Manual

Chapter 1: Introduction

1.1 Rapid Sample Introduction System Standard

Components

The ASXPRESS Rapid Sample Introduction System module cases are made of a

high-strength aluminum alloy with an epoxy powder coating finish. The 6-

port injection valve is constructed of polyphenylene sulphide (PPS), an inert

and dimensionally stable material. The tubing is all inert PTFE (waste tubing

materials may vary by application).

The ASXPRESS system operates reliably under a wide variety of conditions.

Components in the sample flow path are inert, non-metallic materials; when

used at temperatures less than 135°C, they can withstand repeated exposure

to the following substances:

•Predominantly aqueous solutions of strong acids (less than 40%).

•Common organic solvents such as acetone, alcohols, ethyl acetate,

Methylethylketone (MEK), petroleum oils and derived fuels,

tetrachloroethylene, toluene, and xylene.

Prolonged or repeated exposure to temperatures greater than 135°C and to

the following substances can cause failure of the flow path components:

•Solutions of concentrated acids (greater than 40%).

•Partially halogenated hydrocarbons or extremely aggressive organic

solvents (chloroform, methylene dichloride, 1,1,2-trichloroethane).

Figure 1-3 ASXPRESS Rapid Sample Introduction System—Front View.

CAUTION

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