Agilent Technologies 1100 Series Manual de usuario

XCALI-97190 Revision B July 2007

Agilent®1100 Series

LC Devices

Connecting the Hardware and Triggering Data

Acquisition

Agilent®is a registered trademark of Agilent Technologies Inc. Hewlett-Packard®is a registered trademark

of Hewlett-Packard Company. LCQ™, LTQ™, LXQ™, MSQ™, TSQ™, and Xcalibur™are trademarks of

Thermo Fisher Scientific Inc.

Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the

product operation. This document is copyright protected and any reproduction of the whole or any part of this

document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.

The contents of this document are subject to change without notice. All technical information in this

document is for reference purposes only. System configurations and specifications in this document supersede

all previous information received by the purchaser.

Thermo Fisher Scientific Inc. makes no representations that this document is complete, accurate or error-

free and assumes no responsibility and will not be liable for any errors, omissions, damage or loss that might

result from any use of this document, even if the information in the document is followed properly.

This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser. This

document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and Conditions of

Sale shall govern all conflicting information between the two documents.

Release history: First release February 2007, second release July 2007

For Research Use Only. Not regulated for medical or veterinary diagnostic use by U.S. Federal Drug

Administration or other competent authorities.

Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition iii

Preface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .v

About This Guide. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v

Related Documentation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v

Safety and Special Notices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v

Safety Precautions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .vi

Contacting Us . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .vi

Chapter 1 Agilent Modules Supported by LC Devices Versions 2.0.2 and 2.1.0. . . . . . . . . . .1

Chapter 2 Connecting the Hardware . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3

Ethernet Communication Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Installing a Network Card in an Agilent Module. . . . . . . . . . . . . . . . . . . . . . . . . 4

Connecting the Ethernet Communication Cables . . . . . . . . . . . . . . . . . . . . . . . . 7

Installing the External Contact Interface Board . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Connecting the Trigger Cable . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Chapter 3 Configuring the Autosampler for Contact Closure . . . . . . . . . . . . . . . . . . . . . . . . .11

Chapter 4 Triggering Data Acquisition with the Autosampler . . . . . . . . . . . . . . . . . . . . . . . .13

Chapter 5 Turning Off the Solvent Tracking Feature. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15

Appendix A Upgrading an HP 1100 Series LC . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17

Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19

Contents

Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition v

Preface

About This Guide

This guide describes how to hardwire an Agilent®1100 Series LC to a Thermo Scientific

mass spectrometer and the data system computer, configure an Agilent autosampler for

contact closure from within the Xcalibur Instrument Configuration program, and trigger data

collection with an Agilent autosampler.

This guide also describes how to upgrade a Hewlett-Packard®1100 Series LC to an

Agilent 1100 Series LC with Ethernet communication.

Related Documentation

In addition to this guide, Thermo Fisher Scientific provides Help available from within the

Xcalibur software.

Safety and Special Notices

Make sure you follow the precautionary statements presented in this guide. The safety and

other special notices appear in boxes.

Safety and special notices include the following:

CAUTION Highlights hazards to humans, property, or the environment. Each CAUTION

notice is accompanied by an appropriate CAUTION symbol.

CAUTION Highlights electric shock related hazards to human beings. Each electric shock

notice is accompanied by the international High Voltage symbol.

IMPORTANT Highlights information necessary to prevent damage to software, loss of

data, or invalid test results; or might contain information that is critical for optimal

performance of the system.

Preface

vi Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Thermo Scientific

Safety Precautions

To connect the Agilent 1100 Series LC stack to a Thermo Scientific mass spectrometer, you

must install an external contact board in one of the Agilent modules and a LAN interface

board in a second Agilent module. To install a board, you must remove the cover from the

optional board slot. Figure 2 on page 6 shows the location of the slot on the back panel of the

detector.

Before you remove the slot cover from an Agilent 1100 Series module, do the following:

• Turn the power switch to the Off position and unplug the power cable.

• Refer to the Reference Manual for the module for additional safety information and for

information on preventing ESD damage caused by an electrical discharge.

Contacting Us

There are several ways to contact Thermo Fisher Scientific.

YTo contact Technical Support

Find software updates and utilities to download at www.mssupport.thermo.com.

Note Highlights information of general interest.

Tip Helpful information that can make a task easier.

CAUTION To avoid an electric shock, always turn off an Agilent module and unplug

it from line power before you remove its cover.

CAUTION To prevent damage to an instrument, always use ESD protection when

handling electronic boards and components.

Phone 800-685-9535

Fax 561-688-8736

E-mail TechSupport.C+MS@thermofisher.com

Knowledge base www.thermokb.com

Preface

Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition vii

YTo contact Customer Service for ordering information

YTo suggest changes to documentation or to Help

• Fill out a reader survey online at www.thermo.com/lcms-techpubs.

• Send an e-mail message to the Technical Publications Editor at

techpubs.finnigan-lcms@thermofisher.com.

Phone 800-532-4752

Fax 561-688-8731

Web site www.thermo.com/finnigan

Thermo Scientific Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition 1

Agilent Modules Supported by LC Devices

Versions 2.0.2 and 2.1.0

Tab l e 1 lists the model number and firmware versions for the Agilent 1100 Series LC

modules that are supported by the Xcalibur 2.0 and higher data system.

YTo check the firmware version of an Agilent 1100 module

1. Make sure that the Agilent 1100 Series modules are connected by CAN communication

cables, that all the modules are turned on, and that the Agilent 1100 Control Module is

connected.

Refer to the Agilent 1100 Series LC reference manuals for instructions on how to connect

the CAN cables.

2. Press the Esc key on the Control Module until System appears in the upper-left corner of

the LCD display.

3. Press the F4 key on the Control Module to access the Records LCD display.

Table 1. Xcalibur 2.0 supported firmware versions for the Agilent 1100 Series LC

Module Model Number Firmware Version

Binary pump G1312A A.06.01 (012)

Quaternary pump G1311A A.06.01 (012)

Autosampler G1313A A.06.01 (012)

Thermostatted autosampler G1329A A.06.01 (012)

Well-plate autosampler G1367A A.06.01 (012)

Thermostatted column compartment G1316A A.06.01 (012)

Variable wavelength detector G1314A A.06.01 (012)

Diode-array detector G1315A A.06.01 (012)

Multiple wavelength detector*

*Only works with version B of the Control Module.

G1365B A.06.01 (012)

1Agilent Modules Supported by LC Devices Versions 2.0.2 and 2.1.0

2Agilent 1100 Series LC Devices Connecting the Hardware and Triggering Data Acquisition Thermo Scientific

4. Check the firmware versions of the Agilent 1100 Series modules. Refer to Table 1 for the

firmware versions supported by the Xcalibur 2.0. and higher data system.

Records

Module Product Serial# Version On-time EMF

Time Ready

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