Agilent Technologies 8860 Manual de usuario

Agilent Gas Sample Selector for 8860 and 8890

User Manual

Notices

Manual Part Number

G3541-90001

Edition

First Edition, December 2020

No part of this manual may be

reproduced in any form or by any

means (including electronic storage

and retrieval or translation into a

foreign language) without prior

agreement and written consent from

Agilent Technologies, Inc. as governed

by United States and international

Printed in China

Agilent Technologies

(Shanghai) Co., Ltd.

Waigaoqiao Free Trade Zone, Pudong

New Area, Shanghai

412 Yinglun Road

Contact number: (800) 820 3278

Warranty

The material contained in this document

is provided “as is,” and is subject to being

changed, without notice, in future

editions. Further, to the maximum extent

permitted by applicable law, Agilent

disclaims all warranties, either express

or implied, with regard to this manual

and any information contained herein,

including but not limited to the implied

warranties of merchantability and

fitness for a particular purpose. Agilent

shall not be liable for errors or for

incidental or consequential damages in

connection with the furnishing, use, or

performance of this document or of any

information contained herein. Should

Agilent and the user have a separate

written agreement with warranty terms

covering the material in this document

that conflict with these terms, the

warranty terms in the separate

agreement shall control.

Technology Licenses

The hardware and/or software

described in this document are

furnished under a license and may be

used or copied only in accordance with

the terms of such license.

Restricted Rights Legend

U.S. Government Restricted Rights.

Software and technical data rights

granted to the federal government

include only those rights customarily

provided to end user customers.

Agilent provides this customary

commercial license in Software and

technical data pursuant to FAR 12.211

(Technical Data) and 12.212 (Computer

Software) and, for the Department of

Defense, DFARS 252.227-7015

(Technical Data - Commercial Items)

and DFARS 227.7202-3 (Rights in

Commercial Computer Software or

Computer Software Documentation).

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in damage to the product

or loss of important data. Do

not proceed beyond a

CAUTION notice until the

indicated conditions are fully

understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond

a WARNING notice until the

indicated conditions are fully

understood and met.

Agilent Gas Sample Selector for 8860 and 8890 Safety and Installation Manual 3

Contents

1 Safety Information

Safety Information 6

Safety symbols 6

Safety and regulatory information 8

General safety precautions 9

Shipping Instructions 12

Cleaning Instructions 12

Disposal Instructions 12

Intended Use 13

Recycling the Product 13

2 Introduction

Introduction 16

Gas Sample Selector bag version 17

Gas Sample Selector cylinder version 21

Specifications 26

Principle of Operation 28

3 Installation

Before You Begin 32

Installation for Bag Version Gas Sample Selector 33

Shipping kit information (bag version) 33

Site preparation 34

Procedure 35

Installation for Cylinder Version Gas Sample Selector 43

Shipping kit information (cylinder version) 43

Site Preparation 45

4 Agilent Gas Sample Selector for 8860 and 8890 Safety and Installation Manual

Procedure 46

4 Operation

Method Parameters 54

Building a method 54

Programing a sequence 57

Selector Work Flow 59

5 Maintenance and Troubleshooting

Maintenance 62

Replace gas filter for bag version 62

Replace gas filter for cylinder version 66

Sampling mode 70

Purge mode 72

Sweep mode 74

Consumables and parts 76

Troubleshooting 78

Error list for troubleshooting 78

Chromatographic symptoms 79

Restriction and leak check 82

Agilent Gas Sample Selector for 8860 and 8890 Safety and Installation Manual 5

Safety Information

Safety Information 6

Shipping Instructions 12

Cleaning Instructions 12

Disposal Instructions 12

Intended Use 13

Recycling the Product 13

To prevent any injury to the user or any damage to the instrument, it is essential

that you read the information in this chapter and the gas chromatograph (GC)

user manuals.

If this manual is not in your native language, or if you have problems understanding

the text, contact your Agilent office for assistance. Agilent cannot accept

responsibility for any damage or injury caused by misunderstanding of the

information in this manual.

6 Agilent Gas Sample Selector for 8860 and 8890 Safety and Installation Manual

1 Safety Information

Safety Information

Safety symbols

Warnings in the manual or on the instrument must be observed during all phases of

operation, service, and repair of this instrument. Failure to comply with these

precautions violates safety standards of design and the intended use of the

instrument. Agilent Technologies assumes no liability for the customer’s failure to

comply with these requirements.

See accompanying instructions for more information.

Indicates a hot surface.

Indicates hazardous voltages.

Indicates earth (ground) terminal.

Indicates potential explosion hazard.

Indicates electrostatic discharge hazard.

Indicates a hazard.

See the Agilent GC user documentation for the item labeled.

Safety Information 1

Safety symbols

Agilent Gas Sample Selector for 8860 and 8890 Safety and Installation Manual 7

Indicates that you must not discard this electrical/electronic product in

domestic household waste

Manufacturing date.

Power symbol indicates On/Off. The apparatus is not completely

disconnected from the main supply when the power swich is in the Off

position.

8 Agilent Gas Sample Selector for 8860 and 8890 Safety and Installation Manual

1 Safety Information

Safety and regulatory information

The Agilent G3451A Gas Sample Selector conforms to the following safety

standards:

•Canadian Standards Association (CSA): C22.2 No. 61010-1

•CSA/Nationally Recognized Test Laboratory (NRTL): ANSI/UL 61010-1

•International Electrotechnical Commission (IEC): 61010–1, 61010-2-081

•EuroNorm (EN): 61010–1

The Agilent Gas Sample Selector conforms to the following regulations on

electromagnetic compatibility.

•CISPR 11/EN 55011: Group 1, Class A

•IEC/EN 61326-1

NOTE The Gas Sample Selector is designed and manufactured under a quality system

registered to ISO 9001. Declaration of Conformity available.

The Gas Sample Selector meets the following IEC (International Electro-technical

Commission) classifications:

•Safety Class 1

•Transient Overvoltage Category II

•Pollution Degree 2

This unit has been designed and tested in accordance with recognized safety

standards and is designed for use indoors in nonclassified locations. Do not

operate it in an explosive atmosphere. If the instrument is used in a manner not

specified by the manufacturer, the protection provided by the instrument may be

impaired. Whenever the safety protection of the Gas Sample Selector has been

compromised, disconnect the unit from all power sources and secure the unit

against unintended operation. Refer servicing to qualified service personnel.

Substituting parts or performing any unauthorized modification to the instrument

may result in a safety hazard.

Safety Information 1

General safety precautions

Agilent Gas Sample Selector for 8860 and 8890 Safety and Installation Manual 9

Detachable power cord declaration for Japan

㏻ܶ҇瀉朅ࡼ灌炕灢灔灜灡濧㾢牘㓬濧瀅濟ݽ瀭牣濴朅ࡼ灌炕灢灔灜灡瀉

Շ㜐濟瀆濿濟瀁 爽ޯ֡Ӄզ濬娸ռ瀆瀊澝բ㱂濰瀧濺朅ࡼ灌炕灢灔灜灡瀭濥

҄濟濪濻濰濟澞բ㱂濰瀧濺朅ࡼ灌炕灢灔灜灡瀊澝є瀉娸ռ瀂瀊҄牘瀂濨瀙濶

瀮澞

NOTE The power cords are for the Japanese market. Your product must only use the

power cord that was shipped with this product. Do not use this power cord with

any other product.

Sound Emission Certification for Federal Republic of Germany

Sound pressure Sound pressure Lp <70 dB(A) according to DIN-EN 27779.

Schalldruckpegel Schalldruckpegel LP <70 dB(A) nach DIN-EN 27779.

General safety precautions

WARNING When handling or using chemicals for preparation or use within the GC, all

applicable local and national laboratory safety practices must be followed. This

includes, but is not limited to, correct use of Personal Protective Equipment (PPE),

correct use of storage vials, and correct handling of chemicals, as defined in the

laboratory’s internal safety analysis and standard operating procedures. Failure to

adhere to laboratory safety practices could lead to injury or death.

WARNING This instrument is designed for chromatographic analysis of appropriately

prepared samples. It must be operated using appropriate gases, and within

specified maximum ranges for pressure, flows, and temperatures as described in

this manual. If the equipment is used in a manner not specified by the

manufacturer, the protection provided by the equipment may be impaired.

WARNING It is the responsibility of the customer to inform Agilent customer support

representatives if the instrument has been used for the analysis of hazardous

samples, prior to any instrument service being performed or when an instrument

is being returned for repair.

10 Agilent Gas Sample Selector for 8860 and 8890 Safety and Installation Manual

1 Safety Information

General safety precautions

To ensure safe equipment operation, adhere to the following safety practices:

•Dot not use flammable gas (such as H2). Use inert gas (such as N2) instead.

•Perform periodic leak checks on all supply lines and pneumatic plumbing.

•Do not allow gas lines to become kinked or punctured. Place lines away from

foot traffic and extreme heat or cold.

•To avoid exposure to potentially dangerous voltages, disconnect the instrument

from all power sources before removing protective panels.

•Your product must only use the power cord that was shipped with this product.

Do not use this power cord with any other product.

WARNING Replace faulty or frayed power cords immediately. Contact your Agilent service

representative.

•The instrument should be placed in a suitable location with sufficient ventilation

to remove gases. Make sure there is enough space around the instrument for it

to cool off sufficiently.

•Do not turn on the Power Supply if there is a possibility of any electrical

damage. Instead, disconnect the power cord, and contact your Agilent office.

•The supplied power cord must be inserted into a power outlet with a protective

earth ground connection.

•Do not change the external or internal grounding connections as this could

endanger you or damage the Power Supply.

•The Power Supply is properly grounded when shipped. You do not need to

make any changes to the electrical connections or to the Power Supply chassis

to ensure safe operation.

•Do not place containers with flammable liquids on this Power Supply. Spillage

of the liquid over hot parts may cause fire.

•Never try to repair or replace any component that is not described in this

manual without the assistance of an Agilent service engineer. Unauthorized

repairs or modifications will result in rejection of warranty claims.

•Always disconnect the AC power cord before attempting any type of

maintenance.

•The customer should not attempt to replace the fuses in the Power Supply.

•Damage can result if the Power Supply is stored under unfavorable conditions

for prolonged periods (for example, subject to heat, water, and so forth).

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